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Beilstein J. Org. Chem. 2020, 16, 2576–2588, doi:10.3762/bjoc.16.209
Graphical Abstract
Figure 1: Structures of the compounds used in this study: a) crown-8 analogs; b) crown-7 analogs; c) secondar...
Scheme 1: Schematic representation of synthetic routes towards TTFC7, exTTFC7, NDIC7, and NDIC8.
Figure 2: Solid-state structures of a) exTTFC7 (CH3CN molecule omitted for clarity), b) NDIC7 (CH3CN molecule...
Figure 3: a) Synthesis of the [2]rotaxane NDIRot. b) Stacked 1H NMR spectra (700 MHz, CDCl3, 298 K) of NDIC8 ...
Figure 4: UV–vis–NIR spectra obtained by spectroelectrochemical measurements (0.1 M n-Bu4PF6, CH2Cl2/CH3CN 1:...
Beilstein J. Org. Chem. 2018, 14, 1570–1577, doi:10.3762/bjoc.14.134
Scheme 1: (a) Chemical structures of ZB4 and the guests involved in this research. The counterions are PF6−. ...
Figure 1: X-ray single crystal structure of ZB4 and the host–guest complexes. a) ZB4, b) 2+@ZB4-IV, c) 3+@ZB4...
Figure 2: Parabolic free-energy relationship between log(KR/KH) and Hammett parameter σp. KR: guests 11+–21+; ...
Figure 3: X-ray single crystal structures of 14+@ZB4-III, 16+@ZB4-III, 18+@ZB4-III and 21+@ZB4-III. Butyl gro...
Figure 4: X-ray single crystal structures of 18+@ZB4-III and 18+ in 18+@ZB4-III.
Figure 5: Linear relationships of ΔH with temperature (left, slope = −0.13, R2 = 0.9956) and TΔS (right, slop...